Table 2: Accuracy of amino acid analysis.

Amino acid

Asp

Glu

Ser

His

Gly

Thr

Arg

Ala

Tyr

Val

Met

Trp

Phe

Ise

Leu

Lys

 (m/m%)

0.438

2.25

0.375

0.162

0.342

0.241

0.322

0.323

0.231

0.343

0.139

0.092

0.373

0.270

0.550

0.103

X ¯  -  A c

0.026

0.058

0.02

0.01

0.014

0.008

0.032

0.019

0.031

0.030

0.018

0.002

0.016

0.013

0.040

0.015

2 μ B 2  +  μ D 2  

0.042

0.172

0.051

0.027

0.027

0.014

0.054

0.034

0.046

0.030

0.018

0.028

0.028

0.019

0.040

0.036

s

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

A c : Assigned value of the certified reference material (CRM); X ¯ : Mean value obtained for the CRM; μ B 2 : Uncertainty associated with the certified reference value; μ D 2 : Uncertainty associated with the analytical method for the particular analyte; Acceptance criteria: X ¯  -  A c   2 μ B 2  +  μ D 2   ; Asp: Aspartic acid; Glu: Glutamic acid; Ser: Serine; His: Histidine; Gly: Glycine; Thr: Threonine; Arg: Arginine; Ala: Alanine; Tyr: Tyrosine; Val: Valine; Met: Methionine; Trp: Tryptophan; Phe: Phenylalanine; Ile: Isoleucine; Leu: Leucine; Lys: Lysine